Some examples of
environmental experiments under gas and temperature conditions in the
Ly-EtTEM microscope
updated June 06 2015
A
CATALYTIC EXHAUST PIPE in the TEM
Due to European standards
since Euro 4, Diesel Particulate Filters are now compulsory on Diesel
car motors to
diminish Particle Matter emissions through a regeneration phase in
which the collected soot is oxidized. A catalyst, here
Yttria-Stabilised Zirconia is then used to optimize the soot oxidation.
In this low res video sequence recorded at 495°C under 10-2
mbar of oxygen in the EtTEM (full time about 4'), a soot particulate is
consumed at the contact with a ZrO2
crystallite. Magnification is increased at the end of the sequence to
insure atomic resolution; it is seen that some (metallic) impurity
present in this soot synthetized in the laboratory does not burn
[A. SERVE et al., Applied Catalysis
A: General, (2015), online www.elsevier.com/locate/apcata].
Note: the video sequences should run at
a 10 frames-per-seconds speed in nominal conditions (fluent internet
traffic)